1,2-BIS[(DIMETHYLAMINO)DIMETHYLSILYL]ETHANE synthesis
1synthesis methods
- Product Name:1,2-BIS[(DIMETHYLAMINO)DIMETHYLSILYL]ETHANE
- CAS Number:91166-50-6
- Molecular formula:C10H28N2Si2
- Molecular Weight:232.51
the reagent is prepared as a colorless liquid
in 90% yield by treating commercially available bis(chlorodimethylsilyl)
ethane with 5 equiv of dimethylamine in ether at
0°C for 5 h.
13528-93-3
202 suppliers
$6.00/1g
124-40-3
546 suppliers
$18.00/100ml
91166-50-6
69 suppliers
$43.00/2 g
Yield:91166-50-6 90%
Reaction Conditions:
in diethyl ether at 0; for 5 h;
References:
Guggenheim, Thomas L. [Tetrahedron Letters,1984,vol. 25,# 12,p. 1253 - 1254]