1-(4'-NITROPHENYL)-2-TRIMETHYLSILYL ACETYLENE synthesis
- Product Name:1-(4'-NITROPHENYL)-2-TRIMETHYLSILYL ACETYLENE
- CAS Number:75867-38-8
- Molecular formula:C11H13NO2Si
- Molecular Weight:219.31
Yield:75867-38-8 99%
Reaction Conditions:
Stage #1: trimethylsilylacetylenewith piperidine;indium(III) bromide at 20; for 2.5 h;
Stage #2: p-nitrobenzene iodidewith piperidine;[1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II) at 20; for 1 h;
References:
Sakai, Norio;Annaka, Kimiyoshi;Konakahara, Takeo [Organic Letters,2004,vol. 6,# 10,p. 1527 - 1530]
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