2-Aminodiphenylamine synthesis
- Product Name:2-Aminodiphenylamine
- CAS Number:534-85-0
- Molecular formula:C12H12N2
- Molecular Weight:184.24
Yield:534-85-0 71%
Reaction Conditions:
with copper phthalocyanine;copper diacetate in acetonitrile at 15;
Steps:
17 Synthesis of 2-aminodiphenylamine
Reaction flask was added 0.108 g of o-phenylenediamine (1 mmol), phenylhydrazine0.216 g (2 mmol), CuPc 0.058 Ke (0.1 mmol), Cu (OAc) 2 0.02 g (0.1 mmol) and 10 ml ofacetonitrile, 15 °C reaction; TLC until the reaction was followed completely finished;the crude product after the reaction was subjected to column chromatography (petroleumether: ethyl acetate = 100: 1) to give the desired product (71% yield).
References:
WUXI GREEN SEPARATION TECHNOLOGY INST CO LTD;ZOU, JIANPING;JIANG, TAO;ZHOU, SHAOFANG CN104262167, 2016, B Location in patent:Paragraph 0121-0124
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