2-(BENZOTHIAZOL-2-YLSULFANYL)-PROPIONIC ACID synthesis
- Product Name:2-(BENZOTHIAZOL-2-YLSULFANYL)-PROPIONIC ACID
- CAS Number:3383-66-2
- Molecular formula:C10H9NO2S2
- Molecular Weight:239.31
149-30-4
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79-10-7
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3383-66-2
21 suppliers
$57.50/250mg
Yield:-
Reaction Conditions:
with sulfuric acid in water at 45 - 55;Reflux;
Steps:
3
In a four-necked flask equipped with a stirrer, a reflux condenser and a thermometer, 160 ml of 70% sulfuric acid was added, 38 g of 2-mercaptobenzothiazole was added, dissolved in a sulfuric acid solution, and a small amount of 21.2 g Acrylic acid, at 45 ° C to 55 ° C for 2 to 3 hours to produce intermediate compounds; diluted with water, the reaction material, filtration, filter cake with 10% sodium carbonate solution dissolved again filtered to remove insoluble material, the filtrate with dilute sulfuric acid solution Acidified to pH 1 to 2, the target again precipitation, filtration, washing, intermediate compounds were purified.
References:
CN105566391,2016,A Location in patent:Paragraph 0004; 0011
149-30-4
679 suppliers
$5.00/25g
598-78-7
243 suppliers
$9.00/1g
3383-66-2
21 suppliers
$57.50/250mg