3,4'-DIMETHYLBENZHYDROL synthesis
- Product Name:3,4'-DIMETHYLBENZHYDROL
- CAS Number:13389-73-6
- Molecular formula:C15H16O
- Molecular Weight:212.29
625-95-6
255 suppliers
$14.00/25g
104-87-0
520 suppliers
$6.00/25g
13389-73-6
22 suppliers
$500.00/5g
Yield:13389-73-6 95%
Reaction Conditions:
Stage #1: 3-Iodotoluenewith TurboGrignard in tetrahydrofuran at 20;
Stage #2: 4-methyl-benzaldehyde in tetrahydrofuran at 20; under 7757.43 Torr;
Stage #3: with ammonium chloride in tetrahydrofuran;water;
References:
Brodmann, Tobias;Koos, Peter;Metzger, Albrecht;Knochel, Paul;Ley, Steven V. [Organic Process Research and Development,2012,vol. 16,# 5,p. 1102 - 1113] Location in patent:experimental part
13152-94-8
35 suppliers
$497.39/5MG
13389-73-6
22 suppliers
$500.00/5g