3-methylideneoxetane synthesis
- Product Name:3-methylideneoxetane
- CAS Number:10242-62-3
- Molecular formula:C4H6O
- Molecular Weight:70.09
6704-31-0
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Yield:-
Reaction Conditions:
Stage #1:oxetan-3-one;(trimethylsilyl)methylmagnesium chloride in diethyl ether at 0 - 20; for 5 h;Inert atmosphere;Peterson Olefination;
Stage #2: with potassium hydride in tetrahydrofuran at 0 - 20; for 28.75 h;Inert atmosphere;Peterson Olefination;
References:
Green, Samantha A.;Vásquez-Céspedes, Suhelen;Shenvi, Ryan A. [Journal of the American Chemical Society,2018,vol. 140,# 36,p. 11317 - 11324] Location in patent:supporting information
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](http://hg.y866.cn/chemistry/CAS/20210305/GIF/1000210-73-0.gif)
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10242-62-3
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1000210-73-0
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10242-62-3
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