3-PHENYL-2-PROPYN-1-AMINE synthesis
- Product Name:3-PHENYL-2-PROPYN-1-AMINE
- CAS Number:78168-74-8
- Molecular formula:C9H9N
- Molecular Weight:131.17
512785-77-2
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Yield:78168-74-8 96 %
Reaction Conditions:
Stage #1: (3-phenyl-prop-2-ynyl)-carbamic acid tert-butyl esterwith hydrogenchloride in tetrahydrofuran;1,4-dioxane at 20;
Stage #2: with water;sodium hydroxide in tetrahydrofuran;
References:
Ji, Pengwei;Liu, Xiaopei;Xu, Jiwei;Zhang, Xu;Guo, Jianhua;Chen, Wen-Wen;Zhao, Baoguo [Angewandte Chemie - International Edition,2022,vol. 61,# 48,art. no. E202206111][Angew. Chem.,2022,vol. 134,# 48] Location in patent:supporting information
4656-94-4
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78168-74-8
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1504-58-1
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$8.00/1g
78168-74-8
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