4-(CHLOROMETHYL)-2,2-DIMETHYL-1,3-DIOXOLANE synthesis
- Product Name:4-(CHLOROMETHYL)-2,2-DIMETHYL-1,3-DIOXOLANE
- CAS Number:4362-40-7
- Molecular formula:C6H11ClO2
- Molecular Weight:150.6
96-24-2
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$11.00/5g
4362-40-7
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$55.00/5g
Yield: 89%
Reaction Conditions:
with toluene-4-sulfonic acid in acetone
Steps:
1 EXAMPLE 1
EXAMPLE 1 p-Toluenesulfonic acid (1.79 g) was added to a mixture of 3-chloro-1,2-propanediol (104.49 g, 0.945 mol) and acetone (1500 ml) and the resulting mixture was stirred for 12 hours at 25° C. After completion of the reaction, acetone was removed in vacuo and the crude product was distilled to give 128.01 g of 4-chloromethyl-2,2-dimethyl-1,3-dioxolane (yield 89%, b.p. 45° C. at 5 mmHg).
References:
Daiso Co., Ltd. US6143908, 2000, A
100-79-8
403 suppliers
$9.00/25g
4362-40-7
92 suppliers
$55.00/5g