 
            4-Nitropicolinaldehyde synthesis
- Product Name:4-Nitropicolinaldehyde
- CAS Number:108338-19-8
- Molecular formula:C6H4N2O3
- Molecular Weight:152.11
 
                        
                        931-19-1
                        
                        251 suppliers
                        
                        $5.00/5g
                    
 
                        
                        108338-19-8
                        
                        51 suppliers
                        
                        $112.00/100mg
                    
Yield:-
Steps:
                    Multi-step reaction with 4 steps
1: 95 percent / H2SO4, fuming HNO3 / 2 h / 100 - 105 °C
2: 18 percent / Heating
3: 74 percent / aq. NaOH / methanol / 1.5 h / Ambient temperature
4: 66 percent / DMSO, N,N'-dicyclohexylcarbodiimide, H3PO4 / 1.5 h / Ambient temperature
                
References:
Ashimori;Ono;Uchida;Ohtaki;Fukaya;Watanabe;Yokoyama [Chemical and Pharmaceutical Bulletin,1990,vol. 38,# 9,p. 2446 - 2458]
 
                        
                        98197-88-7
                        
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                        $45.00/50mg
                    
 
                        
                        108338-19-8
                        
                        51 suppliers
                        
                        $112.00/100mg
                    
 
                        
                        5470-66-6
                        
                        301 suppliers
                        
                        $8.00/1g
                    
 
                        
                        108338-19-8
                        
                        51 suppliers
                        
                        $112.00/100mg
                    
 
                        
                        36625-64-6
                        
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                        inquiry
                    
 
                        
                        108338-19-8
                        
                        51 suppliers
                        
                        $112.00/100mg
                    
 
                        
                        131747-33-6
                        
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                        108338-19-8
                        
                        51 suppliers
                        
                        $112.00/100mg
                    

 
          

