5'-sulfamoyl-2-chloroadenosine synthesis
- Product Name:5'-sulfamoyl-2-chloroadenosine
- CAS Number:66522-52-9
- Molecular formula:C10H13ClN6O6S
- Molecular Weight:380.76
94482-37-8
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66522-52-9
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: 69 percent / H2 / 5percent Pd/C / toluene; acetic acid / 40 h / Ambient temperature
2: 50 percent / 3M sulfamoyl chloride, CaCO3 / dimethylformamide; CH2Cl2 / 1 h / Ambient temperature
3: 88 percent / 1 h / 120 - 130 °C / under vacuum
4: 63 percent / 20percent NH3 / methanol / 72 h / Ambient temperature
References:
Kristinsson, Haukur;Nebel, Kurt;O'Sullivan, Anthony C.;Struber, Fritz;Winkler, Tammo;Yamaguchi, Yasuchika [Tetrahedron,1994,vol. 50,# 23,p. 6825 - 6838]
103728-78-5
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66522-52-9
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