Benzyl ether synthesis
- Product Name:Benzyl ether
- CAS Number:103-50-4
- Molecular formula:C14H14O
- Molecular Weight:198.26
100-52-7
975 suppliers
$17.30/2g
103-50-4
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$5.00/25g
Yield:103-50-4 98%
Reaction Conditions:
with triethylsilane;silver tetrafluoroborate at 20; for 0.0833333 h;Catalytic behavior;Green chemistry;Reagent/catalyst;Temperature;
Steps:
4 Example 4
Example 4:1% AgBF4 (0.05 mmol, 9.7 mg) was added to the 100 mL reaction flask in turn.Further add benzaldehyde (50 mmol, 5.360 g) and triphenylsilane (50 mmol, 13.6591 g),The reaction was stirred at room temperature for 5 minutes, and after completion of the reaction, direct distillation under reduced pressure (2 mmHg, 90 ° C) gave the desired product.The yield was 98%. The product structure characterization data is the same as in Example 1.
References:
Xuzhou Medical University;Xu Zhou;Liang Ting;Mi Jiajia;Zhai Rongliang;Shi Yanfen CN108164486, 2018, A Location in patent:Paragraph 0043; 0044; 0045; 0046
100-51-6
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103-50-4
325 suppliers
$5.00/25g
120-51-4
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$6.00/25g
100-52-7
975 suppliers
$17.30/2g
100-51-6
1458 suppliers
$5.00/100g
103-50-4
325 suppliers
$5.00/25g
100-44-7
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65-85-0
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103-50-4
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100-39-0
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103-50-4
325 suppliers
$5.00/25g