L-Fucose synthesis
- Product Name:L-Fucose
 - CAS Number:2438-80-4
 - Molecular formula:C6H12O5
 - Molecular Weight:164.16
 
                        
                        79-06-1
                        
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                        2438-80-4
                        
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Yield:2438-80-4 66%
Reaction Conditions:
in water;isopropyl alcohol;
Steps:
                    8 Preparation of polymer 23
Preparation of polymer 23 Monomer 22 (460 mg, 1.44 mmol) and acrylamide (511 mg, 7.21 mmol) were dissolved in 4 mL of pure water and the solution was purged with nitrogen. Then, 5 mg of V-50 initiator was added and the solution was heated to 60° C. The solution became viscous within 30 minutes and heating was stopped. After 24 h, the viscous solution was added to isopropanol dropwise. The polymer was precipitated as a white mass which was filtered and dried in vacuum at room temperature for 48 h. The polymer was obtained as a white solid (640 mg) in 66% yield.
                
References:
US5891862,1999,A
                        
                        212065-83-3
                        
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                        2438-80-4
                        
                        487 suppliers
                        
                        $9.00/250mg
                    
                        
                        7658-10-8
                        
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                        2438-80-4
                        
                        487 suppliers
                        
                        $9.00/250mg