N-(4-Methoxybenzylidene)-N-(4-methoxybenzyl)amine synthesis
- Product Name:N-(4-Methoxybenzylidene)-N-(4-methoxybenzyl)amine
- CAS Number:3261-60-7
- Molecular formula:C16H17NO2
- Molecular Weight:255.31
2393-23-9
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Yield:3261-60-7 100%
Reaction Conditions:
with oxygen;methylene blue;potassium carbonate in acetonitrile at 20; for 10 h;Irradiation;Green chemistry;
Steps:
General Procedure
General procedure: A solution of 4-tert-butylbenzylamine (1a, 0.3 mmol), K2CO3 (3.7 equiv), and MB (1.0 mol%) in dry MeCN (5 mL) in a Pyrex test tube, purged with an O2 balloon, was stirred and irradiated externally with four 22 W fluorescent lamps for 10 h. Products were purified by filtration through a pad of silica gel (3 mm thick) with Et2O, and the filtrate was concentrated.
References:
Okada, Akifumi;Yuasa, Hiroki;Fujiya, Akitoshi;Tada, Norihiro;Miura, Tsuyoshi;Itoh, Akichika [Synlett,2015,vol. 26,# 12,art. no. ST-2015-U0176-L,p. 1705 - 1709]
874-90-8
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123-11-5
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