TRANS-1,2-DIBROMOCYCLOHEXANE synthesis
- Product Name:TRANS-1,2-DIBROMOCYCLOHEXANE
- CAS Number:7429-37-0
- Molecular formula:C6H10Br2
- Molecular Weight:241.95
67-56-1
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5927-93-5
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7429-37-0
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Yield: 64% ， 15%
Reaction Conditions:
with Oxone;ammonium bromide at 20; for 0.0833333 h;stereoselective reaction;
Steps:
General procedure for the synthesis of alkoxybromides
General procedure: To a solution of olefin (2 mmol) in MeOH/EtOH (10 ml) were added NH4Br (2.2 mmol) and oxone(2.2 mmol) and the mixture was stirred at room/reflux temperature for the time shown in Table 2 and 3. After completion (as indicated by TLC), the reaction mixture was filtered and the solvent evaporated under reducedpressure. The products were purified by column chromatography over silica gel.
References:
Kumar, Macharla Arun;Naresh, Mameda;Rohitha, Chozhiyath Nappunni;Narender, Nama [Synthetic Communications,2013,vol. 43,# 23,p. 3121 - 3129] Location in patent:supporting information
110-83-8
321 suppliers
$11.00/25g
7429-37-0
64 suppliers
$18.70/5g
110-83-8
321 suppliers
$11.00/25g
7429-37-0
64 suppliers
$18.70/5g
108-94-1
582 suppliers
$12.00/50g
