TRI-N-BUTYLTIN METHOXIDE synthesis
- Product Name:TRI-N-BUTYLTIN METHOXIDE
- CAS Number:1067-52-3
- Molecular formula:C13H30OSn
- Molecular Weight:321.09
1461-22-9
216 suppliers
$10.00/10g
124-41-4
730 suppliers
$12.00/25g
1067-52-3
94 suppliers
$49.20/25g
Yield:1067-52-3 80%
Reaction Conditions:
in toluene for 6 h;Reflux;
Steps:
2.2. Synthesis of Bu3SnOR initiators
General procedure: Tributyltin alkoxides (Bu3SnOR; R = Me, Et, nPr and nBu) weresynthesized by the nucleophilic substitution of tributyltin chloride(Bu3SnCl) by sodium alkoxides (NaOR; R = Me, Et, nPr and nBu) inanhydrous toluene at reflux conditions for 6 h as described inliterature [14,25]. The synthesized Bu3SnOR were purified byvacuum distillation and the chemical structure was identified byproton nuclear magnetic resonance spectroscopy (1H NMR) on aBruker Avance 400 NMR Spectrometer operating at 400 MHz inchloroform-d (CDCl3) and Fourier transform infrared spectroscopy(FT-IR) on a Bruker Tensor 27 FT-IR spectrometer.
References:
Limwanich, Wanich;Khunmanee, Sureerat;Kungwan, Nawee;Punyodom, Winita;Meepowpan, Puttinan [Thermochimica Acta,2015,vol. 599,p. 1 - 7]
67-56-1
790 suppliers
$7.30/5ml-f
688-73-3
190 suppliers
$13.00/1g
1067-52-3
94 suppliers
$49.20/25g
616-38-6
719 suppliers
$5.00/5 g
56-35-9
191 suppliers
$30.00/100 g
1067-52-3
94 suppliers
$49.20/25g
67-56-1
790 suppliers
$7.30/5ml-f
24850-33-7
198 suppliers
$12.00/5g
1067-52-3
94 suppliers
$49.20/25g
![Stannane, tributyl[(methoxycarbonyl)oxy]- (9CI)](http://hg.y866.cn/chemistry/CAS/20200515/GIF/17207-78-2.gif)
17207-78-2
0 suppliers
inquiry
124-38-9
134 suppliers
$175.00/23402
1067-52-3
94 suppliers
$49.20/25g