Z-ILE-VAL-OH synthesis
- Product Name:Z-ILE-VAL-OH
 - CAS Number:41487-00-7
 - Molecular formula:C19H28N2O5
 - Molecular Weight:364.44
 
                        
                        72-18-4
                        
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Yield:-
Steps:
                    Multi-step reaction with 4 steps
1: 85 percent / thionylchloride / Ambient temperature
2: 85 percent / triethylamine, chloroformic acid ethyl ester / CH2Cl2 / 1) -10 deg C, 1 h, 2) 2 h, room temperature
3: NaI / acetone
4: Zn, HgCl2 / acetone / 48 h / Heating
                
References:
Buchholz, Michael;Kunz, Horst [Liebigs Annalen der Chemie,1983,# 11,p. 1859 - 1885]
                        
                        3160-59-6
                        
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                        88962-27-0
                        
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