翻译翻译,我又来了O(∩_∩)O~
At point B the pattern obtained corresponds to an amorphous product on which enlarged peaks, slightly shifted towards larger angles, corresponding to nickel nitrate dihydrate are visible. At point C the pattern obtained is essentially that of an amorphous product with some peaks, mostly in the background noise, due to nickel nitrate dihydrate. These peaks are even more displaced to higher angles than those observed at point B. Furthermore a significant small angle diffusion can be noted. At point D, the pattern obtained corresponds well to the anhydrous nickel nitrate. At points E and F, the patterns observed correspond to nickel oxide. It can be noticed however that the peaks are narrower for the product isolated at higher temperature. At 5 mbar (Fig. 3a), the pattern shows peaks corresponding to several species including nickel nitrate hexahydrate, tetrahydrate, dihydrate and the anhydrous nitrate. At point b, the spectrum includes peaks corresponding to nickel nitrate tetrahydrate and dihydrate. At point c, the spectrum obtained corresponds to that of a basic salt with the following composition: Ni(NO3)2, .2Ni(OH)2. The pattern of the product isolated at point d shows small peaks corresponding to nickel nitrate tetrahydrate and dihydrate. More significant peaks are also observed from anhydrous nickel nitrate and nickel oxide whose peaks are shifted towards larger diffraction angles. At point e, the spectrum obtained corresponds to nickel oxide with peaks of smaller width than the oxide obtained at 5 X IO-2 mbar.
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At point B the pattern obtained corresponds to an amorphous product on which enlarged peaks, slightly shifted towards larger angles, corresponding to nickel nitrate dihydrate are visible. 在B点获得的晶体结构相当于一个非晶体产品,在其上可以看见与硝酸镍二水合物相关的扩大的高峰,轻微移动的大角度。At point C the pattern obtained is essentially that of an amorphous product with some peaks, mostly in the background noise, due to nickel nitrate dihydrate. These peaks are even more displaced to higher angles than those observed at point B. Furthermore a significant small angle diffusion can be noted. 在C点获得的晶体结构基本上是一些带高峰的非晶产品,主要是在背景噪音下,由于硝酸镍二水合物引起的。这些高峰中比B点更多的转移到高角度,另外可以看到一个重要小角度扩散。At point D, the pattern obtained corresponds well to the anhydrous nickel nitrate. At points E and F, the patterns observed correspond to nickel oxide. It can be noticed however that the peaks are narrower for the product isolated at higher temperature.在D点获得的晶体结构与无水硝酸镍很相符。点E和F ,获得的晶体结构与氧化镍相符。不管怎样,可以注意到,孤立在较高的温度的产品高峰更窄。 At 5 mbar (Fig. 3a), the pattern shows peaks corresponding to several species including nickel nitrate hexahydrate, tetrahydrate, dihydrate and the anhydrous nitrate. At point b, the spectrum includes peaks corresponding to nickel nitrate tetrahydrate and dihydrate. At point c, the spectrum obtained corresponds to that of a basic salt with the following composition: Ni(NO3)2, .2Ni(OH)2. 在5毫巴的余压下 (图3A ),晶体结构显示出与包括六水硝酸镍,四水合物,二水合物和无水硝酸盐在内的几个物种一致。在B点,光谱包括与四水硝酸镍和二水硝酸镍一致的高峰。在C点,获得的光谱相当于含以下成分的基本盐:Ni(NO3)2, .2Ni(OH)2.。The pattern of the product isolated at point d shows small peaks corresponding to nickel nitrate tetrahydrate and dihydrate. More significant peaks are also observed from anhydrous nickel nitrate and nickel oxide whose peaks are shifted towards larger diffraction angles. 在D点分离出的晶体结构显示出与四水硝酸镍和二水硝酸镍相符的小高峰。从峰值转向更大的衍射角的无水硝酸镍和氧化镍中,还观察到更重要的高峰。At point e, the spectrum obtained corresponds to nickel oxide with peaks of smaller width than the oxide obtained at 5 X IO-2 mbar. 在E点获得的光谱与氧化镍相符,其宽度比在5 ×IO - 2 毫巴的余压下获得的氧化氮要小。
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B点的方式获得相当于非晶产品上扩大高峰,稍有大角度转向,相当于硝酸镍二水可见。在C点的格局基本上是获得的非晶产品与一些高峰,主要是在背景噪音,由于硝酸镍二水。这些山峰更流离失所比更高的角度观察点湾另外一个重要小角度扩散可以看到。在D点,对应的模式获得良好的无水硝酸镍。点E和F ,观察到的模式相对应的氧化镍。它可以发现然而,该山峰是狭义的产品更高的分离
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一楼只给你翻译了前面 翻译的还不错,下面我来补充, 在5 mbar (图3A )条,高峰期的格局显示相应的一些物种,包括硝酸镍六,四水,二水和 无水硝酸盐。 B点,频谱包括高峰相应硝酸镍四水和二水。在C点,得到的频谱 相当于一个基本盐组成如下:镍( NO3 ) 2的, 0.2镍( OH ) 2的。模式的产品孤立点D显示相应的小高峰硝酸镍四水和二水。更重要的山峰也观察到无水硝酸镍和氧化镍,其峰值转向更大的衍射角。点英,频谱获得相当于氧化镍峰较小宽度比氧化氮获得5 ×的IO - 2 mbar 。
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在B点模式得到一种无定形的产品与增加的山峰,大角度,轻微转向二相对应的镍硝态氮是可见的。在C语言模式,取得一种无定形的产品有些山峰,大多在背景噪音,由于二镍硝态氮。这些山顶更加转移给更高的角度观察到b点比另外一个显著的小角度扩散可以指出。在D点对应的模式,取得良好的无镍硝酸盐。在E和F、模式与镍氧化物。观察然而,它能被注意到的山峰在产品窄孤立较高 温度。 5标称(图3a),对应于数种显示峰,包括镍硝酸盐hexahydrate tetrahydrate、二水和 无硝态氮。在这样的事上、光谱峰对镍相应包含tetrahydrate硝态氮和人员。在c的光谱 相对应的一个基本的盐以下列组成:镍硝态氮.2Ni(哦),(2)。这个图案的产品在d点分离相对应的小峰显示tetrahydrate硝态氮和二镍。更有意义的山峰也观察到无镍硝态氮和镍氧化物的山峰都转向更大的衍射角度。在市场上,获得相当于镍氧化物频谱宽度与滞后于洪峰的小比5×IO-2氧化物标称。
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