95984-11-5 (N-(2,2-二甲氧基乙基)甲基丙烯酰胺,N-(2,2-Dimethoxyethyl)-2-methylpropenamide)

_90%

反应条件：

1.1 Reagents: Dicyclohexylcarbodiimide , N-Hydroxysuccinimide Solvents: Tetrahydrofuran ; 2 h, cooled
1.2 Reagents: Triethylamine Solvents: Tetrahydrofuran ; cooled; rt; 3 d, rt

参考文献：

Paramagnetic solid supports with coating of synthetic copolymer for use as assay reagents

, World Intellectual Property Organization, , ,

合成路线：1 步

79-41-4

_90%

反应条件：

1.1 Reagents: Dicyclohexylcarbodiimide , N-Hydroxysuccinimide Solvents: Tetrahydrofuran ; 2 h, cooled
1.2 Reagents: Triethylamine Solvents: Tetrahydrofuran ; rt; 3 d, rt

参考文献：

Composition for use as an assay reagent

, World Intellectual Property Organization, , ,

合成路线：1 步

_89%

反应条件：

1.1 Reagents: Triethylamine Solvents: Dichloromethane ; 3 h, < 10 °C

参考文献：

Saccharide-derived monomers, curable compositions therefrom, and aqueous compositions therefrom for jet-printing inks

, Japan, , ,

合成路线：1 步

反应条件：

1.1 Reagents: Sodium hydroxide Catalysts: Tempo Solvents: Water ; 2 h, 10 °C; 24 h, rt

参考文献：

Poly(oligoethylene glycol methacrylate) hydrogel compositions, and methods of use thereof

, United States, , ,

合成路线：1 步

反应条件：

1.1 Reagents: Sodium hydroxide Catalysts: Tempo Solvents: Water ; 2 h, 10 °C; 24 h, 10 °C → rt

参考文献：

Method for the preparation of degradable microgel particles using a stimuli-responsive prepolymer, and microgel compositions thereof

, United States, , ,

合成路线：1 步

反应条件：

1.1 Reagents: Sodium hydroxide , Tempo Solvents: Water ; 2 h, 10 °C; 24 h, rt

参考文献：

Temperature-Induced Assembly of Monodisperse, Covalently Cross-Linked, and Degradable Poly(N-isopropylacrylamide) Microgels Based on Oligomeric Precursors

Sivakumaran, Daryl; Mueller, Eva; Hoare, Todd, Langmuir, 2015, 31(21), 5767-5778

合成路线：1 步

反应条件：

1.1 Reagents: Sodium hydroxide , Tempo Solvents: Water ; 10 °C; 2 h, 10 °C; 24 h, rt

参考文献：

Injectable and tunable poly(ethylene glycol) analogue hydrogels based on poly(oligoethylene glycol methacrylate)

Smeets, Niels M. B.; Bakaic, Emilia; Patenaude, Mathew; Hoare, Todd, Chemical Communications (Cambridge, 2014, 50(25), 3306-3309

合成路线：1 步

反应条件：

1.1 Reagents: Sodium hydroxide , Tempol Solvents: Water ; 2 h, 0 °C; 0 °C → rt; overnight, rt

参考文献：

Tuning Gelation Time and Morphology of Injectable Hydrogels Using Ketone-Hydrazide Cross-Linking

Patenaude, Mathew; Campbell, Scott; Kinio, Dennis; Hoare, Todd, Biomacromolecules, 2014, 15(3), 781-790

合成路线：1 步

反应条件：

1.1 Reagents: Triethylamine Solvents: Acetone ; 3 h, 0 °C

参考文献：

Organic solvent-soluble polyvinyl acetals capable of forming crosslinked structures with good solvent resistance, and their powder coatings and ceramic binders

, Japan, , ,

合成路线：1 步

反应条件：

1.1 Reagents: Sodium hydroxide , Tempol Solvents: Water ; 3.5 h, 10 °C; pH 7.2

参考文献：

Method and composition for incorporating radiation-absorbing agents into polymers

, United States, , ,

合成路线：1 步