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Concomitant polymorphism and supramolecular isomerism in 1,3,5-tris(4-cyanobenzoyl)benzene
V. S. Senthil Kumar,F. Christopher Pigge,Nigam P. Rath
New Journal of Chemistry Pub Date : 09/22/2003 00:00:00 , DOI:10.1039/B307492G
Abstract

The title compound, 1,3,5-tris(4-cyanobenzoyl)benzene, exhibits the phenomenon of concomitant polymorphism. Two distinct isomeric solid-state networks, honeycomb and ladder, were obtained upon crystallization from acetone–water solution. Conformational flexibility of the molecule appears to facilitate polymorph formation. Each network is maintained via formation of multiple C–H⋯N and C–H⋯O hydrogen bonds.

Graphical abstract: Concomitant polymorphism and supramolecular isomerism in 1,3,5-tris(4-cyanobenzoyl)benzene
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