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“Isothermal” LCST transitions triggered by bioreduction of single polymer end-groups†‡
Matthew J. Summers,Daniel J. Phillips,Matthew I. Gibson
Chemical Communications Pub Date : 07/06/2012 00:00:00 , DOI:10.1039/C2CC34236G
Abstract

The α-termini of RAFT-derived thermoresponsive polymers were functionalised via thiol exchange with pyridyl disulfide. Addition of hydrophilic end-groups dramatically increased the observed cloud point of the polymers, without changing the composition of the main chain. Selective cleavage of the disulfide-linked end-groups was observed under conditions intended to mimic intracellular glutathione concentration. This allowed the thermoresponsive behaviour to be ‘switched on’ without the need for a temperature stimulus – an ‘isothermal’ switch.

Graphical abstract: “Isothermal” LCST transitions triggered by bioreduction of single polymer end-groups
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