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Colorimetric detection of chemical warfare simulants†
Karl J. Wallace,Jeroni Morey,Vincent M. Lynch,Eric V. Anslyn
New Journal of Chemistry Pub Date : 09/22/2005 00:00:00 , DOI:10.1039/B506100H
Abstract

Two simple chromogenic indicators (4) and (5), containing different supernucleophilic moieties, have been synthesized. Upon phosphorylation with two chemical warfare agent (CWA) simulants, a hypsochromic shift of approximately 50 nm is observed in an NaOH–DMSO solution. The oximate supernucleophile was found to be a better supernucleophile than the hydrazone moiety. Two X-ray crystal structures were obtained from unexpected synthetic side products obtained in this study. These will also be discussed.

Graphical abstract: Colorimetric detection of chemical warfare simulants
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