960化工网
Crystal structures and solid-state fluorescence of BODIPY dyes based on Λ-shaped Tröger's base†
He Xi,Chun-Xue Yuan,Ye-Xin Li,Yang Liu,Xu-Tang Tao
CrystEngComm Pub Date : 01/12/2012 00:00:00 , DOI:10.1039/C2CE06260G
Abstract

Two Λ-shaped BODIPY dyes based on Tröger's base, 2,8-(6H,12H-5,11-methanodibenzo[b,f]diazocineylene)-di(4,4-difluoro-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene) (DFTMB) and 2,8-(6H,12H-5,11-methanodibenzo[b,f]diazocineylene)-di(4,4-difluoro-2,6-diethyl-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene) (DFDEB), were designed and synthesized. Both compounds exhibit intense fluorescence in dilute solution and polycrystalline powder form. From the crystal structure, the impact of the substitutions at the BODIPY core on the crystal packing mode, intermolecular π–π interactions and optical behavior is compared and discussed. The results indicate that the close π–π stacking in the crystalline state has been effectively inhibited by the twisted Λ-shaped Tröger's base.

Graphical abstract: Crystal structures and solid-state fluorescence of BODIPY dyes based on Λ-shaped Tröger's base
平台客服
平台客服
平台在线客服