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13C isotopomics of triacylglycerols using NMR with polarization transfer techniques†
Joseph Bejjani,Toufic Rizk,Virginie Silvestre,Gerald S. Remaud,Serge Akoka
Analytical Methods Pub Date : 05/21/2015 00:00:00 , DOI:10.1039/C5AY01250C
Abstract

A rapid and very precise method is proposed to simultaneously determine the position-specific 13C content and the metabolomic profile of triacylglycerols (isotopomics). 13C-NMR spectra are obtained by using an adiabatic INEPT sequence; the experiment time is reduced by a factor of 7 with respect to a one-pulse acquisition.

Graphical abstract: 13C isotopomics of triacylglycerols using NMR with polarization transfer techniques
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