Efficient synthesis of 3,4-ethylenedioxythiophenes (EDOT) by Mitsunobu reaction
Dolores Caras-Quintero,Peter Bäuerle
Chemical Communications Pub Date : 10/16/2002 00:00:00 , DOI:10.1039/B207640C
Abstract

Using the Mitsunobu reaction as a key step, a general and efficient method for the synthesis of EDOT monomers has been developed. Novel substituted EDOTs and the first chiral derivatives were generated in high yields.

Graphical abstract: Efficient synthesis of 3,4-ethylenedioxythiophenes (EDOT) by Mitsunobu reaction