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Introduction of useful peripheral functional groups on [2]catenanes by combining Cu(i) template synthesis with “click” chemistry†
Jackson D. Megiatto, Jr.,David I. Schuster
New Journal of Chemistry Pub Date : 11/11/2009 00:00:00 , DOI:10.1039/B9NJ00486F
Abstract

Two protocols based on Cu(I) template synthesis and “click” reactions for the synthesis of functionalized [2]catenanes are described. A straightforward procedure, involving high dilution conditions at high temperatures (70 °C), affords [2]catenanes bearing two identical peripheral groups in high yields. For the preparation of non-symmetrically functionalized [2]catenanes, a second milder and simpler protocol was developed, generalizing and extending the method. The introduction of peripheral functional groups into the catenane structure opens up possibilities of using [2]catenanes as building blocks for preparation of even more complex structures.

Graphical abstract: Introduction of useful peripheral functional groups on [2]catenanes by combining Cu(i) template synthesis with “click” chemistry
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