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In situ TEM observation of the structural transformation of rutile TiO2 nanowire during electrochemical lithiation†
Sung Joo Kim,Sun-Young Noh,Alireza Kargar,Deli Wang,George W. Graham,Xiaoqing Pan
Chemical Communications Pub Date : 07/09/2014 00:00:00 , DOI:10.1039/C4CC04161E
Abstract

We present the first direct experimental proof that phase changes occur during the real-time lithiation of rutile TiO2 nanostructures, functioning as the anode of a solid Li-ion battery inside a transmission electron microscope.

Graphical abstract: In situ TEM observation of the structural transformation of rutile TiO2 nanowire during electrochemical lithiation
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