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A robust, sensitive, and versatile HMBC experiment for rapid structure elucidation by NMR: IMPACT-HMBC†
Julien Furrer
Chemical Communications Pub Date : 04/01/2010 00:00:00 , DOI:10.1039/C000964D
Abstract

A robust, versatile and easy to optimize HMBC experiment for complex organic structure elucidation which has been experimentally tested on cholesteryl acetate, cyclosporine and isopropylidene glycerol is described. The proposed experiment, IMPACT-HMBC (improved and accelerated constant-time heteronuclear multiple-bond correlation), combines sensitivity, easy experimental setup and can be recorded with short recovery times.

Graphical abstract: A robust, sensitive, and versatile HMBC experiment for rapid structure elucidation by NMR: IMPACT-HMBC
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