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One-pot structural conversion of magadiite into MFI zeolitenanosheets using mononitrogensurfactants as structure and shape-directing agents†
T. Jean Daou,Nicolas Bats,Bogdan Harbuzaru,Grégory Lapisardi,Hélène Chaumeil,Albert Defoin,Loïc Rouleau,Joël Patarin
CrystEngComm Pub Date : 02/11/2013 00:00:00 , DOI:10.1039/C3CE40118A
Abstract

MFI-type materials with a lamellar morphology were successfully synthesized by using mononitrogen surfactants specifically designed by molecular modelling. The mononitrogen surfactants directed the recrystallization of a crystalline layered polysilicate formed in situ, the magadiite, into a zeolite ZSM-5. Moreover, the surfactants allow the preservation of the lamellar shape of the magadiite and inhibit a further growth into one dimension, leading to the formation of zeolite ZSM-5 nanosheets with a thickness comprised between 2 and 3 nm and a Si/Al ratio of 24. This simple approach paves a new way for obtaining zeolite materials of controlled size and shape for specific catalytic applications.

Graphical abstract: One-pot structural conversion of magadiite into MFI zeolite nanosheets using mononitrogen surfactants as structure and shape-directing agents
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