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Chiral phosphine-squaramide-catalyzed Morita–Baylis–Hillman reaction: enantioselective synthesis of 3-hydroxy-2-oxindoles†
Jing-Ying Qian,Ci-Ci Wang,Feng Sha
RSC Advances Pub Date : 05/31/2012 00:00:00 , DOI:10.1039/C2RA20521A
Abstract

Phosphine-squaramide derivatives were developed to catalyze the enantioselective Morita–Baylis–Hillman reaction of acrylates with isatins to construct 3-hydroxy-2-oxindoles with quaternary stereocenters. In the presence of 2 mol% H–bonding catalyst 3e, the desired products were achieved in high yields and good-to-excellent enantioselectivities (up to 95% ee).

Graphical abstract: Chiral phosphine-squaramide-catalyzed Morita–Baylis–Hillman reaction: enantioselective synthesis of 3-hydroxy-2-oxindoles
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