960化工网
Synthesis of quaternary stereogenic centres via stereoselective intermolecular Friedel–Crafts reactions†
Jennifer C. Ball,Robert Gleave,Simon Jones
Organic & Biomolecular Chemistry Pub Date : 04/20/2011 00:00:00 , DOI:10.1039/C1OB05129F
Abstract

Highly stereoselective Friedel–Crafts reactions have been performed using a chiral anthracene template to control the selectivity of the reaction. In the case of additions to fully substituted N-acyliminium ions, competitive elimination and condensation reactions were observed. Retro-Diels–Alder reaction of one of the reaction products led to a precursor that could be used for the construction of pyroglutamic acids bearing quaternary stereogenic centres.

Graphical abstract: Synthesis of quaternary stereogenic centres via stereoselective intermolecular Friedel–Crafts reactions
平台客服
平台客服
平台在线客服