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Transition metal free, green and facile halogenation of ketene dithioacetals using a KX–oxidant system†‡
Vishakha Rai,Ganesh Shivayogappa Sorabad,Mahagundappa Rachappa Maddani
New Journal of Chemistry Pub Date : 01/04/2021 00:00:00 , DOI:10.1039/D0NJ03737K
Abstract

A facile oxidative halogenation of α-oxo ketene dithioacetals is achieved by using a potassium halide and oxidant combination under transition metal free conditions at ambient temperature. Using this methodology, halogenated ketene dithioacetals are synthesized in good to excellent yields with a short reaction time. The halogenated products are successfully transformed into nitrogen containing heterocyclic molecules.

Graphical abstract: Transition metal free, green and facile halogenation of ketene dithioacetals using a KX–oxidant system
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