Trapping of benzene oxide-oxepin and methyl-substituted derivatives with 4-phenyl- and 4-pentafluorophenyl-1,2,4-triazoline-3,5-dione
Alistair P. Henderson,Esra Mutlu,Amélie Leclercq,Christine Bleasdale,William Clegg,Richard A. Henderson,Bernard T. Golding
Chemical Communications Pub Date : 08/01/2002 00:00:00 , DOI:10.1039/B205079J
Abstract
4-Phenyl-1,2,4-triazoline-3,5-dione and its pentafluoro analogue are efficient reagents for trapping arene oxides, e.g. benzene oxide-oxepin, affording crystalline adducts that can be quantitatively analysed by HPLC and MS techniques.