The synthesis of the largest perfluoro macrocycles;
perfluoro [60]-crown-20 and perfluoro [30]-crown-10Electronic supplementary
information (ESI) available: experimental details. See
http://www.rsc.org/suppdata/cc/b0/b004168h/
Han-Chao Wei,Richard J. Lagow
Chemical Communications Pub Date : 10/16/2000 00:00:00 , DOI:10.1039/B004168H
Abstract
The largest perfluoro macrocycles, perfluoro [60]-crown-20 and perfluoro [30]-crown-10, have been synthesized using the new continuous addition solution phase direct fluorination technique and characterized using 19F NMR and mass spectrometry.
