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One pot synthesis of fluorescent π-conjugated materials: immobilization of phenylene–ethynylene polyelectrolytes in silica confined ionogels†
Nathalie Cheminet,Thibaut Jarrosson,Jean-Pierre Lère-Porte,Françoise Serein-Spirau,Luiz Cury,Joel Moreau,Lydie Viau,André Vioux
Journal of Materials Chemistry Pub Date : 08/01/2011 00:00:00 , DOI:10.1039/C1JM11733E
Abstract

Phenylene–ethynylene monomer and copolymer bearing pendant imidazolium groups were synthesized in order to obtain luminescent entities highly soluble in ionic liquids (ILs). Their stabilities under non-aqueous sol–gel conditions (i.e. using formic acid) allowed their incorporation into silica in the form of ionogels. This was performed in a one step synthesis and the resulting materials were found to be easily processable as monoliths and showed interesting luminescent properties. Given the high solubility of 2,4-dinitrotoluene in the investigated IL, (1-butyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide), the relevance of these ionogels as luminescent sensors was tested.

Graphical abstract: One pot synthesis of fluorescent π-conjugated materials: immobilization of phenylene–ethynylene polyelectrolytes in silica confined ionogels
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