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Asymmetric synthesis of chiral cyclic amine from cyclic imine by bacterial whole-cell catalyst of enantioselective imine reductase†
Koichi Mitsukura,Mai Suzuki,Kazuhiro Tada,Toyokazu Yoshida,Toru Nagasawa
Organic & Biomolecular Chemistry Pub Date : 08/12/2010 00:00:00 , DOI:10.1039/C0OB00353K
Abstract

Streptomyces sp. GF3587 and 3546 were found to be imine-reducing strains with high R- and S-selectivity by screening using 2-methyl-1-pyrroline (2-MPN). Their whole-cell catalysts produced 91 mM R-2-methylpyrrolidine (R-2-MP) with 99.2%e.e. and 27.5 mM S-2-MP (92.3%e.e.) from 2-MPN at 91–92% conversion in the presence of glucose, respectively.

Graphical abstract: Asymmetric synthesis of chiral cyclic amine from cyclic imine by bacterial whole-cell catalyst of enantioselective imine reductase
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