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Mass spectrometry in structural and stereochemical problems. Part CLXXV. Evidence against electron impact-induced alkyl shifts in the mass spectra of α-hydroxy-ketones
Journal of the Chemical Society C: Organic Pub Date : , DOI:10.1039/J39690002550
Abstract

Recently the mass spectra of simple α-hydroxy-ketones were reported to contain peaks arising from isomeric ketols attributed to electron impact-induced 1,2-alkyl migrations. These peaks have now been shown to be an artifact of thermal rearrangements in the inlet systems. The mass spectra of simple tertiary ketols from A.E.I. model MS-9 and Finnigan model 1015 mass spectrometers are compared and contrasted.

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