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Azabenzocycloheptenones. Part IX. A new synthesis and some reactions of the 5,6-dihydrodibenz[b,e]azepin-11-one system
Journal of the Chemical Society C: Organic Pub Date : , DOI:10.1039/J39690001321
Abstract

Cyclisation of N-(m-methoxybenzyl)-N-tosylanthraniloyl chloride with aluminium chloride at –20° yielded 5,6-dihydro-8-methoxy-5-tosyldibenz[b,e]azepine-11-one (70%), which could be detosylated with polyphosphoric acid. Some reactions of the dihydrodibenzazepinone system are described.

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