Crystal structure and conformation of 1-phenyl-4,4-dimethoxyphosphorinan
Journal of the Chemical Society D: Chemical Communications Pub Date : , DOI:10.1039/C29710001020
Abstract
The title compound is shown by X-ray analysis to have a chair conformation with an axial phenyl substituent; the 1H n.m.r. spectrum is consistent with one preferred conformation in solution, and 31P and 13C chemical shifts are also reported.