Chirality direct co-crystallization of different configurationally opposite dialkyl 2,5-diazabicyclo[2.2.2]octane-3,6-dione-1,4-dicarboxylates,10.1070/MC1999v009n04ABEH001120

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Chirality direct co-crystallization of different configurationally opposite dialkyl 2,5-diazabicyclo[2.2.2]octane-3,6-dione-1,4-dicarboxylates

Mendeleev Communications Pub Date : , DOI:10.1070/MC1999v009n04ABEH001120

Abstract

The title procedure gives quasi-racemic optically active (CD) co-crystals of 4 (space group P2₁) and 5 of the 1:1 composition; in [CD(–)230]-4, molecules of (–)-1 and (+)-2 are joined by amide H-bonds into infinite linear zigzag tapes packed as infinite columns.

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