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期刊名称:Surface Topography: Metrology and Properties
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Characterization of aperiodic surfaces with mesh-based parameters
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-06-12 , DOI: 10.1088/2051-672x/acd868
StefanieStöckel,FrankSegel,SophieGroeger
For technical surfaces, it is important to know their functional purpose and to characterize them accordingly. Therefore, ISO 21920–2 in 2D and ISO 25178–2 in 3D offer parameters that can assess surface functional properties. The topographic portions of a surface, for example hills and dales, can be classified as features and evaluated using feature parameters. However, no parameter exists to describe the spatial distribution of features with regard to the degree of homogeneity for aperiodic surfaces. Here we show the application of the Delaunay triangulation to quantify the spatial distribution respectively the geometric relationship of features. Therefore, the feature points are determined by watershed analysis and the resulting point cloud is meshed in 2D. Based on that mean and standard deviation of the triangle side lengths and the area disorder (AD) are calculated as new parameters. The method is demonstrated for sandblasted and chrome-plated specimens. In addition simulation is used to generate more data for analysis. With the proposed approach the distinction and extent of uniform, homogeneous or inhomogeneous spatial distributions of features with parameter AD can be determined.
Experimental analysis of anodic coating process parameters of Al 5754 alloy by response surface method
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-06-08 , DOI: 10.1088/2051-672x/acdaaf
IlhanCelik,FatihErdemir,IsaCoruhlu
Aluminum 5754 alloy appears as a candidate material for many engineering applications in terms of its lightness and strength values. The surface properties of this alloy need to be improved for applications where there is surface damage such as friction and wear. In this study, Central composite design was applied to investigate the influences of anodic coating process parameters (voltage, coating time and grit size) on the response (i.e. surface roughness and coating thickness). The competence of the mathematical models recognized, and the importance of the regression coefficients were studied by ANOVA. The initial surfaces of the samples were sanded with 400, 800 and 1200 grit size and surfaces with 3 different roughnesses were obtained. Al 5754 specimens were anodic coated at 8 V, 12 V and 16 V voltages and combinations of time parameters of 10, 20 and 30 min The ANOVA results show that the designed models by RSM for average coating thickness and surface roughness are statistically important at the confidence level of 95%, and 80%, respectively. Maximum anodic coated layer of 29 μm was obtained at surface prepared with 1200 grit size, at 16 V of voltage and used for 30 min of anodizing time. The lowest roughness value of 0.676 μm was obtained at the surface was prepared with 1200 grit size, 8 V of voltage and anodizing time of 10 min.
Effect of graphene dispersed coconut biodiesel on the Micro ED milling characteristics of Inconel 718 alloy
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-05-31 , DOI: 10.1088/2051-672x/acd79a
KVArunPillai,PSaravanaKumar
Micro Electrical discharge milling is a familiar micromachining process for machining of complex microstructures using a cylindrical tool. In this research work, the influence of process parameters namely capacitance, voltage, threshold on response indicators during machining of Inconel 718 with coconut biodiesel and graphene nano powder dispersed coconut biodiesel is investigated in detail. Further, surface-topography of the machined surface was critically examined using scanning electron microscopy and three-dimensional non-contact roughness tester. Graphene nano powder concentration (0.3 g l−1) increased the MRR around 68% compared to coconut biodiesel (BD). A medium order of capacitance (10 nF) offered a maximum MRR irrespective of dielectric used. With higher order capacitance, the minimum TWR is obtained due to longer pulse off duration. High surface finish is achieved with graphene nano powder dispersed coconut BD due to uniformly distributed of craters on the machined surface. Recast layer thickness is 3.08 μm, 1.62 μm and 2.34 μm with coconut biodiesel, 0.3 g l−1 and 0.6 g l−1 graphene particles mixed coconut biodiesel, respectively. Minimum recast layer is observed with graphene particles mixed coconut biodiesel under considered parametric conditions due to lesser eroded particle deposition. EDS results confirm that the sedimentation of graphene nano powder (increase in carbon %) on work surface results in increase in hardness. Crater size, voids and cracks were reduced with graphene nano powder dispersed coconut BD due to uniform distribution of heat energy over machining region. Results showed that the graphene nano powder mixed coconut biodiesel can be the substitute for mineral oil.
A review on TIG cladding of engineering material for improving their surface property
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-05-30 , DOI: 10.1088/2051-672x/acd6aa
KaushikBiswas,ChinmayaKumarSahoo
Different components used in industries like power plant, petrochemical, automobile are subjected to severe wear and corrosion due to high temperature and pressure environments. Therefore, it is necessary to improve those components’ wear and corrosion resistance properties. Different processes like laser cladding, CVD, PVD, and thermal spraying are widely used for upgrading surface properties of material. In recent days, it has been found that many researchers investigated the performance of tungsten inert gas (TIG) welding for cladding of superior material like ceramics, metal etc on different substrate materials. TIG cladding can fulfil the requirements of industries by developing a quality cladded layer with low cost and high productivity. This research paper has made an effort to compile the literature related to TIG cladding process for improving substrate properties. It has been observed that the superior materials like titanium carbide(TiC), silicon carbide(SiC), tungsten carbide(WC), cobalt-based alloys, and nickel-based alloys have been successfully cladded using TIG welding process. Researchers have also observed adequate improvement in properties like microhardness and wear resistance of different grades of steel substrate material, like 304, 316 stainless steel, 1010, and 1020 low-carbon steel. The process is also successfully utilized for cladding of superior material on nonferrous metals like Al, Ti alloy. The TIG clad quality and performance rely on different process parameters like current, scan speed, and shielding gas flow rate and also the properties of coating and substrate material.
An overview on plasma-assisted thermochemical treatments of martensitic stainless steels * * A preliminary version of this manuscript was presented at 2nd International Conference on Surface Engineering in Material Forming, October 2-4, 2019, Porto Alegre-RS, Brazil.
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-01-27 , DOI: 10.1088/2051-672x/acb372
CristianoJoséScheuer,RodrigoPeritoCardoso,SilvioFranciscoBrunatto
Demand for higher wear and corrosion resistance components has attracted increasing interest in surface engineering. This line of research develops alternative processes for improving the surface properties of engineering materials. The traditional route seeks the development of new alloys. However, the cost and time associated with these developments become prohibitive in many cases. Currently, the application of plasma-assisted thermochemical treatments has been a technically and economically viable alternative to extend the lifespan of components exposed to severe environments. In this sense, the tooling industry is one of the oldest and most traditional users of plasma-assisted processes, since forming, injection and/or cutting tools are usually subjected to wear and corrosion degradation. Among the various materials used to make tools, we highlight the martensitic stainless steels, which are used in the manufacture of molds and inserts for injection of chlorinated and fluorinated thermoplastic and thermoset polymers. In these applications, martensitic stainless steels are exposed to severe deterioration conditions due to abrasive wear and corrosion by chloride and fluoride ions. Considering the variety of available plasma-assisted thermochemical treatments whose application allows improving metallic materials corrosion and wear resistance, it is a complex task to select the better process and its execution parameters to ensure the maximum performance in operation. In this work, it is proposed a systematic method to aid the process selection task, focused on thermochemical treatments of martensitic stainless steels, which integrates the processing conditions and the resulting microstructure, properties and performance. For this purpose, working envelop for selecting processes and processing parameters were elaborated, that allow qualify and quantify the correlations among each specific plasma-assisted thermochemical treatment (like nitriding, carburizing, nitrocarburizing, etc.) execution conditions, with the resulting properties and performance for treated martensitic stainless steels. In parallel, the genesis of plasma-assisted thermochemical treatments is also described, a bibliometric analysis is carried out on the publications on the subject, and also, a summary description of the surface characteristics of the treated materials is realized.
Synthesis and characterisation of single and duplex ZnO/TiO2 ceramic films on additively manufactured bimetallic material of 316L stainless steel and Ti6Al4V
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-05-17 , DOI: 10.1088/2051-672x/accf6c
TYetim,HTekdir,MTaftalı,KTuralıoğlu,AFYetim
Selective laser melting (SLM), one of the Laser Powder Bed Fusion (LPBF) additive manufacturing methods, has enabled the layered production of Ti6Al4V/316L layered samples, thanks to the layer-by-layer construction. Although 316L and Ti6Al4V are used in many engineering applications, their wear performance is limited. This study aims to improve the tribological and electrochemical properties of Ti6Al4V/316L layered samples. Thus, ZnO, TiO2 monolayer, composite, and ZnO/TiO2, TiO2/ZnO multilayer ceramic films on Ti6Al4V/316L layered surface sample, were coated via the sol-gel dip-coating process. The structural, morphological, and tribological properties of ZnO-TiO2 ceramic films were analyzed via x-ray diffractometer, Scanning Electron Microscopy (SEM), and 3D profilometer. The tribological properties of these coatings were examined using a reciprocating tribo-tester, and the electrochemical properties of samples were evaluated through potentiodynamic polarization and electrochemical impedance spectroscopy measurements. Structural and mechanical results indicated that ZnO and TiO2 films (monolayer, composite, and multilayer-coated) have higher surface roughness and hardness values than additively manufactured Ti6Al4V/316L layered models. Both single and multilayer ZnO and TiO2 ceramic-coated films improved the wear resistance of the Ti6Al4V/316L substrate. Also, The best tribological and corrosion resistance was acquired for the multilayer film (ZnO/TiO2) among all the coated models.
Effects of growth temperature on structural and electrical properties of in-rich InAlN–GaN heterostructures by radio-frequency metal–organic molecular beam epitaxy
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-04-27 , DOI: 10.1088/2051-672x/acce51
Wei-ChunChen,Kun-AnChiu,Hung-PinChen,Yu-WeiLin,Che-ChinChen,Fong-ZhiChen
In-rich InAlN is a promising nitride semiconductor alloy for high-efficiency solar cells and wide-range light-emitting diodes due to its tunable bandgap from 0.7 to 6.2 eV. However, incomplete characterization has led to inconsistent fundamental properties in some studies. The aim of this study was to comprehensively investigate the structural, optical, and electrical properties of In-rich InAlN films grown on GaN/Al2O3 templates by RF-MOMBE at various temperatures. The methodology involved state-of-the-art metrology techniques, such as high-resolution x-ray diffraction (HRXRD), scanning electron microscopy (FE-SEM), Hall effect measurements, and transmission electron microscopy (TEM). The results showed that all InxAl1-xN films were epitaxially grown on the GaN/Al2O3 template, with the indium composition (x) decreasing with increasing growth temperature. Furthermore, phase separation of the In-rich InAlN films occurred at high growth temperatures(>550 °C), resulting in a relatively smooth surface. The optical absorption method measured the band-gap of the InxAl1-xN films, which ranged from 1.7 to 1.9 eV for x values between 0.77 and 0.91. The mobility and carrier concentrations of all In-rich InAlN films were measured at ∼60−277 cm2 V−1-s−1 and 2–7 × 1019 cm3 in the growth temperature of range 450 °C–610 °C, respectively. In conclusion, our comprehensive characterization using advanced metrology methods provides valuable insights into the properties of In-rich InAlN films, which can inform future optimization of these materials for various applications.
Fractal and statistical characterization of brushstroke on paintings
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-03-28 , DOI: 10.1088/2051-672x/acbe53
MaxenceBigerelle,RobinGuibert,AnnaMironova,FredericRobache,RaphaelDeltombe,LudovicNys,ChristopherABrown
Identification of an individual artist’s touch on paintings is studied using surface metrology. Paintings’ topographies were measured using focus variation and stitching, creating 13 × 13 mm maps with 1 μm sampling intervals, and 169 megapixels, with a 10X objective lens. Topographic characterization parameters were analyzed for their ability to differentiate different painters’ renderings. Statistical treatments from data mining were used to discriminate, by optimization, multiscale topographic signatures characterized by a multitude of areal texture parameters. It appears that a fractal dimension can define 3 characteristic scale ranges. One from 3 to 70 μm corresponds to brushstroke details. Another, from 70 to 700 μm, corresponds to the topography of the material of the canvas fabric. Finally, scales greater than 700 μm correspond to undulations of the canvas. For scales less than 50 μm, the fractal structure of the topography left by brushstrokes follows a power law characterized by the slopes of the topography. The topography of the clouds painted on the canvas has an Sdq (topographic slopes) increasing with the clarity of the clouds at scales of 3–500 μm. According to the Torrance-Sparrow theory, the higher the Sdq, the more diffuse the light on the surface. The painter therefore wanted to show, by his brushstroke, that the light clouds diffuse more light giving an impression of local brightness. This study is confirmed by the analysis of the painting of Max Savy, a French painter from Carcassonne (1918–2009), which was measured with a white light interferometer Zygo NewView 7300, a X100 objective lens giving a 517 μm × 517 μm stitched surface, with a sampling interval of 0.109 μm. The box-counting method for estimating the fractal dimension of the topography of an oil painting appears optimal by the fact that it morphologically integrates scale variations of the local slopes of the surface morphology. This method thus characterizes the multiscale aspects, as well as the scale changes, of the topography.
Deposition processing and surface metrology of MoNx thin films by design of experiment and single variable (nitrogen flow rate) methods
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-03-22 , DOI: 10.1088/2051-672x/acc088
Fong-ZhiChen,I-ShengTing,Wei-ZenKang,Yu-WeiLin,Jia-HongHuang
In this study, the Taguchi design of experiment (DOE) was performed to optimize the deposition process of MoNx thin films using unbalanced magnetron sputtering (UBMS). Further single-variable experiments based on the sensitive parameter derived from the Taguchi experiments were conducted to investigate the effect of the parameter on the phase evolution, structure, and properties of the MoNx thin films. The MoNx thin films were deposited using DC-UBMS. Four controlling factors: N2 flow rate, substrate bias voltage, substrate temperature, and substrate rotational speed were selected in the Taguchi L9 matrix experiment. Electrical resistivity and hardness were chosen as the quality characteristics for the optimization. Analysis of variance (ANOVA) and analysis of mean (ANOM) were performed to identify the sensitive parameters and the optimum conditions. The confirmation test results for the optimizations of hardness (SH) and electrical resistivity (SR) were within the predicted ranges, and therefore the feasibility and reliability of the Taguchi optimization were verified. The results of ANOVA showed that nitrogen flow rate was the most sensitive factor. The optimum condition for the electrical resistivity was chosen to be the reference for the single-variable experiments, and nitrogen flow rate was selected as the controlling variable. The MoNx specimens in the single-variable experiment showed prevailing (200) texture that could be attributed to the lowest surface energy associated with (200) plane and the base metal steering effect by Mo (110). The results of single-variable experiments indicated that the retained Mo metal phase played an important role in hardness, electrical resistivity, and residual stress.
Quality assurance of stereolithography based biocompatible materials for dental applications
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-03-07 , DOI: 10.1088/2051-672x/acbe54
AmoghVKrishna,VijethVReddy,DyallWDexter,Dan-ÅkeWälivaara,PeterAbrahamsson,B-GRosen,JonasAnderud
Additive Manufacturing (AM) is increasingly being used in healthcare sectors for its potential to fabricate patient-specific customized implants, and specifically in dentistry, AM finds its applications in maxillofacial implants, dentures, and other prosthetic aids. However, in most applications, AM is largely being used for prototyping purposes. The full-scale realization of AM can only be achieved if the downsides of AM are addressed and resolved. Hence this paper focuses on providing a detailed analysis of surface quality, dimensional accuracy, and mechanical properties of the biocompatible material produced, using the Stereolithography (SLA) method for a dental application. For quality analysis, test artefacts were produced, and the quality was assessed before and after the sterilization process. The results suggest that micro-surface roughness essential for cell growth is similar for all build inclinations and well within the control limit required for effective bone regeneration. Multi-scale surface characterization revealed that the sterilization process involving heat can potentially alter the micro-roughness features of resin-based materials. The results from the dimensional analysis show that the SLA parts produced had negligible dimensional deviations from the CAD model to the printed parts and were unaffected by the sterilization process. The tensile test results suggest that the part orientation does not affect the tensile strength and that the sterilization process seems to have an insignificant effect on the tensile properties of the SLA parts. Furthermore, the results were validated by producing a membrane barrier for Guided Bone Regeneration (GBR). The validation results showed that excess resin entrapment was due to the geometrical design of the membrane barrier. In conclusion, this paper provides an overview of quality variations that can help in optimizing the AM and sterilization process to suit dental needs.
On communicating extruded aluminium surface quality along the supply chain – a customer approach to sustainable surfaces
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-03-27 , DOI: 10.1088/2051-672x/acc544
SRebeggiani,MBergman,B-GRosén,LEriksson
Today, far too many products are scrapped due to surface related issues, products with perfect function but with minor surface blemishes. The complaints are often offset by goodwill commitments from suppliers at great cost to them and delivery delays and lead time costs for customers. The reason is that the industry relies on several non-standardized classification systems for surface quality that are based on various combinations of and designations for surface defects, assessed by visual inspections at a defined distance to determine the severity of any detected surface deviations. These similar classification systems provide far too much scope for subjective and non-repeatable assessments causing communication problems between customer and producer at all stages in the supply chain. To challenge this situation, a common toolbox to communicate, describe and define surface quality should be developed, i.e. a standardisation of surface quality assessment including various effects and defects with a jointly established nomenclature and evaluation parameters. This work presents the first step of a research project bringing together 11 suppliers and OEMs along the supply chain, from the delivery of raw aluminium to finished alumina profiles included in consumer products. The final goal of the project is to develop an ‘objective classification of visual requirements’ on alumina profiles towards increased sustainability and decreased material wastage. Presented result is a common terminology with links to the process chain, surface defect geometry and visual appearance aiming at making the communication between producers and buyers of the aluminium profiles clearer and more unambiguous when it comes to specification and requirements of profile surfaces in each of the supply-chain links. Future work will add measurable parameters specifying surface quality.
Comparison of the wear behavior and surface properties of zirconia and resin-based CAD/CAM restorative materials after different sandblasting procedures
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-02-10 , DOI: 10.1088/2051-672x/acb8cd
SevalBaşpınarAlper,NeslihanTekçe,SinanFidan,SibelBalcı
Objective: To evaluate the effects of different sandblasting procedures on the wear and surface properties of zirconia and resin-based CAD/CAM restorative materials and to evaluate the relationships among materials and procedures. Materials and Methods: A total of 160 specimens of 2 mm thickness were prepared from Cerasmart, Vita-Enamic, Tetric-CAD, and Katana-Zirconia CAD/CAM materials. Each material was divided into four groups. Group-1: Control; Group-2: 29 μm Al2O3; Group-3: 30 μm CoJet; and Group-4: 50 μm Al2O3. Sandblasting procedures were applied from a distance of 10 mm for 15 s at 2 bar pressure. The volume loss resulting from sandblasting was calculated. The samples were then scanned with a Nanovea-PS50 non-contact profilometer. The Ra, Rz, and Sa values were recorded. The data were analyzed with the Shapiro-Wilk test and two-way ANOVA. Results: Group-4 showed the highest Ra and Rz values in all materials. The highest Sa and volume differences values were observed for Cerasmart, Vita-Enamic, and Tetric-CAD in Group-4; similar values were obtained for Katana-Zirconia. When the materials were compared, Cerasmart exhibited the highest volume differences, Ra, Rz, and Sa values in Group-4, while Katana-Zirconia demonstrated the lowest. Conclusions: Sandblasting procedure and material type showed a significant impact on the wear and surface properties. The abrasive effect increased with the increasing Al2O3 particle sizes for resin-matrix materials. Sandblasting with 50 μm Al2O3 exhibited the lowest wear and surface roughness values for Katana-Zirconia and the highest for Cerasmart.
Elevated-temperature wear behavior of Ti6Al4V alloy: microstructural evolution and properties change in subsurfaces and mild-severe wear transition
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-01-31 , DOI: 10.1088/2051-672x/acb564
JAn,SGZhang,DHDu,HXChen
Dry sliding wear behavior of Ti6Al4V alloy was studied at elevated temperatures of 50 °C–400 °C. The constituent phases and morphologies of worn surfaces were examined to evaluate the roles of oxide layers and wear mechanisms in mild-severe wear transition (M-SWT). Microstructural evolution and hardness change in subsurfaces were also investigated to reveal the most fundamental reason for M-SWT. The results showed that M-SWT happened via severe plastic deformation (SPD) within 20 °C–350 °C, while mild wear prevailed via a protective mechanically mixed layer (MML) containing multiple oxide phases at 400 °C. Large surface plastic deformation and frictional heat activated dynamic recrystallization (DRX) softening in subsurface, which resulted in M-SWT. The critical load for M-SWT presented an approximate linear relationship with testing temperature within 20 °C–250 °C, from which a critical temperature of 555.8 °C for M-SWT was obtained by linearly fitting method. It was thought as the critical temperature for DRX realization in surface layer, and it was utilized to calculate the transition loads at 300 °C and 350 °C.
Effect of texture on hydrodynamic journal bearing performance under starvation lubrication
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-01-23 , DOI: 10.1088/2051-672x/acaac0
HeLi,JunkaiNiu
The effect of texture on tribological properties of journal bearings operating under starvation lubrication conditions is studied in this paper. The P-θ model with mass conservation boundary conditions is used to accurately predict the oil film distribution in the full oil film/starvation region of the textured bearing. The effects of various degrees of starvation lubrication on the tribological performance parameters, such as eccentricity, attitude angle, full film area, and friction coefficient, are discussed in textured bearings. The results show that the effect of texture on the bearing performance is affected by starvation lubrication conditions: (1) The effect severity varied with starvation levels; (2) The texturing still improved the operating performance of the journal bearing in the case of weak starvation; (3) Texturing increased the bearing load carrying capacity and reduced the friction coefficient, improving safety and preventing safety accidents due to oil supply problems.
Effects of argon plasma pretreatment of Si wafers on Si-Si bonding based on Mo/Au interlayers
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-05-22 , DOI: 10.1088/2051-672x/acd569
YongfengQu,HaiyangBai,WenboHu,YuanYuan,ShengliWu,HongxingWang,HuiqingFan
To improve the bonding quality of Si-Si wafers bonded based on Mo/Au intermediate layers at room temperature, the surfaces of Si wafers were pretreated with argon plasma, and the effect of argon plasma pretreatment on Si-Si wafer bonding was analyzed by combining experimental and theoretical methods. Owing to the plasma treatment of Si wafers, the surface roughness of Si wafers was significantly reduced, and the bonded Si-Si samples had lower interfacial voidage. The average bonding strength of 11.46 MPa for the argon plasma pretreated Si-Si bonded samples is much higher than the bonding strength of 4.23 MPa for the unpretreated Si-Si bonded samples. The analysis of the fractured surface revealed that the fracture of the Si-Si bonded samples without argon plasma treatment occurred mainly at the Mo/Si interface, while the fracture of the plasma-treated Si-Si bonded samples arose mainly within the bulk Si. Molecular dynamics (MD) simulations suggest that strong atomic diffusion takes place at the Mo/Au interface, while Mo atoms hardly diffuse into the bulk Si. These results indicate that argon plasma pretreatment not only cleans and activates the Si wafer surface but also makes the Si wafer surface smooth, which helps to enhance the deposited Mo/Au film quality and the adhesion between the Mo film and the Si wafer.
Effects of surface topography through laser texturing on the surface characteristics of zirconia-based dental materials: surface hydrophobicity, antibacterial behavior, and cellular response
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-05-05 , DOI: 10.1088/2051-672x/acd076
ArashGhalandarzadeh,MonirehGanjali,MiladHosseini
The continuous need for high-performance implants that provide significant biological properties has led to extensive research into the topographic patterns of bioceramics in recent years. Their excellent aesthetics, biocompatibility, low plaque affinity, and ability to reproduce a natural-looking appearance have contributed to their success in dentistry. 3 mol% Yttria-stabilized zirconia (3YSZ) is gaining popularity as a material for dental implants due to its excellent mechanical properties and minimal degradation when exposed to body temperature. However, such materials show limited biological and antibacterial performance for dental applications. The purpose of this work was to develop microtopographies on the surface of 3YSZ ceramic by laser ablation technique, in order to improve its biological response and antibacterial behaviors. Two types of microtextures, including micro-grooves and micro-channels geometries were fabricated onto the zirconia ceramics using the laser ablation technique. The effects of different microtextures on the wettability, biological and antibacterial behaviors of 3YSZ ceramics were studied. The results indicate that all of the microstructure patterns are capable of improving the performance of 3YSZ. Wettability is a decisive factor that determines the antibacterial performance of textured zirconia ceramics. The microtextured surfaces all display hydrophobic behavior, thus yielding an effective improvement of antibacterial performance for 3YSZ ceramics. Cell-surface interactions were assessed for 7 days on both zirconia textured surfaces and a nontextured control with pre-osteoblast MC3T3-E1 cells. The obtained results showed the positive influence of textured zirconia surfaces on cell biological response.
Non-integral model-based scatterometry for CD metrology of single high-aspect-ratio microstructures
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-05-05 , DOI: 10.1088/2051-672x/acd0c5
Wei-HsinChein,Fu-ShengYang,Zi-YingFu,Liang-ChiaChen
This article presents an innovative model-based scatterometry method for CD metrology of single high-aspect-ratio (HAR) microstructures, which are increasingly utilized in advanced packaging, especially as vertical interconnects in three-dimensional integrated circuits. The rapidly growing aspect ratio of these HAR structures makes it challenging to monitor their critical dimensions (CD). Furthermore, conventional spectral reflectometry or scatterometry measurements on periodic metrology targets on the scribe lines of the wafer are inadequate in providing a reliable correlation with the in-die structures due to the integral nature of these measurements, which can result in additional measurement errors compared to measuring individual in-die structures. To address these challenges, we propose a novel scatterometry system that can achieve high-precision single-structure measurement of fine-pitch HAR structures with significantly improved light efficiency over conventional optical methods. Our system takes advantage of the high spatial coherence of the supercontinuum laser source and an optical NA-controlled design concept for precise light beam shaping, enabling high spatial resolution and superior light efficiency in measurements. Furthermore, we demonstrate a model-based measurement scheme that uses a virtual optical system for complete characterization of the sample profile. The experimental results show that the proposed system can accurately measure RDL structures with fine nominal spacing as small as 1 μm and an aspect ratio of 3:1 with high fidelity.
Effects of surface roughness and counter body variables on the dry sliding wear behavior of AISI 4140 steel based on the elastoplastic flattening model
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-04-13 , DOI: 10.1088/2051-672x/accafe
YılmazKüçük,AzmiErdoğan,BilalKurşuncu,MSabriGök
This study aimed to determine the effect of surface roughness and counter body material on the wear behavior of AISI 4140 steel based on the elastoplastic flattening model. Most studies in tribology based on the elastoplastic regime focus on modeling the contact between a sphere and a flat surface. However, these models’ main challenge is determining the real contact area. This study claims that the real contact area can be detected with high accuracy through interface software used in optical microscopy. The sample surfaces were roughened and then supposed to dry sliding wear tests using the AISI 52100 and Al2O3 abrasive counter bodies under varying loads and test durations. It was concluded from the calculations that the sample’s surface roughness value significantly affects the contact pair’s plasticity index and, thus, the sample’s wear behavior against the counter body material. Higher plasticity index values indicating the abrasive effect were obtained with the Al2O3 ball, which has a higher hardness and elasticity modulus than the AISI 52100 steel ball. The surface damage of the sample with a high roughness value was less than the other samples. The COF values obtained with the steel ball were detected as lower than that of the alumina ball. Also, it was seen that the surface roughness parameter and plasticity index values calculated were compatible with the wear characteristics of the test samples. As a result, determining the real contact area between the contacting surfaces and its usability in calculating the elastoplastic flattening model parameters were experimentally tested and verified.
Silicone implant surface roughness, friction, and wear
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-03-20 , DOI: 10.1088/2051-672x/ac9f5a
DixonJAtkins,AllisonLChau,JonahMRosas,Yen-TsungChen,SamanthaTChan,JuanManuelUrueña,AngelaAPitenis
Some textured silicone breast implants with high average surface roughness (‘macrotextured’) have been associated with a rare cancer of the immune system, Breast Implant-Associated Anaplastic Large Cell Lymphoma (BIA-ALCL). Silicone elastomer wear debris may lead to chronic inflammation, a key step in the development of this cancer. Here, we model the generation and release of silicone wear debris in the case of a folded implant-implant (‘shell-shell’) sliding interface for three different types of implants, characterized by their surface roughness. The ‘smooth’ implant shell with the lowest average surface roughness tested (Ra = 2.7 ± 0.6 μm) resulted in average friction coefficients of μ avg = 0.46 ± 0.11 across 1,000 mm of sliding distance and generated 1,304 particles with an average particle diameter of D avg = 8.3 ± 13.1 μm. The ‘microtextured’ implant shell (Ra = 32 ± 7.0 μm) exhibited μ avg = 1.20 ± 0.10 and generated 2,730 particles with D avg = 4.7 ± 9.1 μm. The ‘macrotextured’ implant shell (Ra = 80 ± 10 μm) exhibited the highest friction coefficients, μ avg = 2.82 ± 0.15 and the greatest number of wear debris particles, 11,699, with an average particle size of D avg = 5.3 ± 3.3 μm. Our data may provide guidance for the design of silicone breast implants with lower surface roughness, lower friction, and smaller quantities of wear debris.
The investigation of wear properties of nanoparticle-reinforced epoxy composite material surfaces
Surface Topography: Metrology and Properties ( IF 0 ) Pub Date : 2023-05-19 , DOI: 10.1088/2051-672x/acd4d4
SerkanApay,MertKilinçel
This study added nano-sized Al2O3, Boron, and TiO2 powders to the epoxy polymer at 0.5% and 1% ratios. Abrasive wear resistance properties of nanoparticle-reinforced epoxy polymers were investigated. First cylindrical specimens with and without additives were prepared for realizing the experimental research. Pin-on discs were used for the wear test of epoxy samples. The mass losses were measured via a precision scale. According to the results, the boron nanoparticles have increased the epoxy specimens’ resistance. As a result of the experimental studies, it was observed that the wear resistance of the epoxy composite increased with each nano-sized powder added to the epoxy. SEM and optical profilometry investigated the composites’ friction coefficient and surface morphology. As a result of friction coefficient and wear weight loss tests, the highest wear resistance was obtained in 1% boron powder nano-reinforced epoxy composites. It was observed that the epoxy friction coefficient was in the range of 0.4–0.6, which decreased to the range of 0.2–0.4 with the addition of nano boron. The surface roughness value after epoxy wear was measured as 1.4 μm. With the addition of nano boron, this value was measured as 0.32 μm. Optical profilometry and SEM imaging results also support these values.
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自引率H-indexSCI收录状况PubMed Central (PML)
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