934545-80-9 (3-溴-9-(2-萘基)咔唑,3-Bromo-9-(naphthalen-2-yl)-9H-carbazole)

_93%

反应条件：

1.1 Reagents: Potassium carbonate Catalysts: 1,10-Phenanthroline , Cuprous iodide , 18-Crown-6 Solvents: Dimethylformamide ; overnight, rt → reflux

参考文献：

Preparation of heterocyclic compounds for organic electroluminescent devices

, China, , ,

合成路线：1 步

_85%

反应条件：

1.1 Catalysts: Tributylphosphine , Tris(dibenzylideneacetone)dipalladium Solvents: Toluene , Water ; 12 h, rt

参考文献：

Organic light-emitting devices and displays with emitting layers employing multiple hosts

, United States, , ,

合成路线：1 步

34292-03-0

_84%

反应条件：

1.1 Reagents: N-Bromosuccinimide Solvents: Tetrahydrofuran ; 20 h, rt

参考文献：

Hole transport materials and organic electroluminescent devices using them

, Korea, , ,

合成路线：1 步

34292-03-0

_83%

反应条件：

1.1 Reagents: N-Bromosuccinimide Solvents: Dimethylformamide ; 4 h, rt

参考文献：

Novel organic electroluminescent compounds having high luminous efficiency for improved driving lifespan and greater efficiency in electroluminescent devices, and organic electroluminescent devices comprising the organic electroluminescent compounds

, World Intellectual Property Organization, , ,

合成路线：1 步

_79%

反应条件：

1.1 Reagents: Potassium carbonate Catalysts: Copper , 18-Crown-6 Solvents: Dimethylformamide ; 24 h, 140 °C; 140 °C → rt
1.2 Reagents: Hydrochloric acid Solvents: Water ; 30 min, rt

参考文献：

Preparation of carbazole compounds for electronic device

, World Intellectual Property Organization, , ,

合成路线：1 步

580-13-2

_78%

反应条件：

1.1 Reagents: Sodium tert-butoxide Catalysts: Tris(dibenzylideneacetone)dipalladium , 2-Dicyclohexylphosphino-2′,6′-dimethoxybiphenyl Solvents: Toluene ; rt → 108 °C; 3 h, 108 °C

参考文献：

Adamantyl-containing carbazole-type organic compounds, organic electroluminescent device and electronic device comprising the same

, China, , ,

合成路线：1 步

_73%

反应条件：

1.1 Reagents: Potassium carbonate , Sodium sulfate Catalysts: Copper Solvents: Nitrobenzene ; 200 °C

参考文献：

Amine based hole transport layer and carbazole-based light emitting auxiliary layer for organic electroluminescent device

, Korea, , ,

合成路线：1 步

_69%

反应条件：

1.1 Reagents: Sodium tert-butoxide Catalysts: Tri-tert-butylphosphine , Tris(dibenzylideneacetone)dipalladium Solvents: o-Xylene ; 16 h, 135 - 140 °C

参考文献：

Preparation of (dibenzofuranyl)indolo[2,3-b]carbazole derivatives as organic light emitting layer and its applications in OLEDs

, China, , ,

合成路线：1 步

34292-03-0

_66%

反应条件：

1.1 Reagents: N-Bromosuccinimide Catalysts: Benzoyl peroxide Solvents: Dichloromethane ; 12 h, rt

参考文献：

New bipolar green host materials containing benzimidazole-carbazole moiety in phosphorescent OLEDs

Park, Jung Hwan; Kim, Eun Kyung; El-Deeb, Ibrahim M.; Jung, Su Jin; Choi, Dae Hyuk; et al, Bulletin of the Korean Chemical Society, 2011, 32(3), 841-846

合成路线：1 步

580-13-2

86-74-8

_65%

反应条件：

1.1 Reagents: Potassium carbonate , Cuprous iodide Catalysts: 18-Crown-6 Solvents: 1,3-Dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone ; 5 h, reflux; reflux → rt
1.2 Reagents: Water ; rt; 30 min, rt
1.3 Reagents: N-Bromosuccinimide Solvents: Dimethylformamide ; 40 min, 0 °C; overnight, rt
1.4 Reagents: Water

参考文献：

preparation of 1,2-benzo[a]anthracene derivatives as organic electroluminescent materials

, China, , ,

合成路线：1 步

580-13-2

反应条件：

1.1 Reagents: Potassium carbonate Catalysts: 1,10-Phenanthroline , Cuprous iodide Solvents: Dimethylformamide ; 16 h, 150 °C

参考文献：

Organic electroluminescence device and amine compound for organic electroluminescence device

, United States, , ,

合成路线：1 步

反应条件：

1.1 Reagents: Potassium carbonate Catalysts: Copper Solvents: Toluene ; rt → 150 °C; 24 h, 150 °C

参考文献：

Preparation of anthracene-based compounds useful as electroluminescent material in OLED

, China, , ,

合成路线：1 步

反应条件：

1.1 Reagents: Potassium acetate Catalysts: 1,10-Phenanthroline , Cuprous iodide Solvents: Dimethylformamide ; 18 h, rt → reflux

参考文献：

Two organic host materials for organic optoelectronic element and display device

, World Intellectual Property Organization, , ,

合成路线：1 步

反应条件：

1.1 Reagents: Potassium carbonate , Sodium sulfate Catalysts: Copper Solvents: Nitrobenzene ; 200 °C

参考文献：

Heteroaryl compounds as organic electronic device materials

, World Intellectual Property Organization, , ,

合成路线：1 步

反应条件：

1.1 Reagents: Potassium carbonate Catalysts: 1,10-Phenanthroline , Cuprous iodide Solvents: Xylene ; 6 h, reflux

参考文献：

Preparation of phosphindolo[2,3-b]carbazole 7-oxide derivatives for organic electroluminescent devices

, Korea, , ,

合成路线：1 步

反应条件：

1.1 Reagents: Sodium tert-butoxide Catalysts: Copper , 18-Crown-6 Solvents: Toluene ; 24 h, 100 °C

参考文献：

Azacarbazole compounds as organic electronic device materials

, World Intellectual Property Organization, , ,

合成路线：1 步

反应条件：

1.1 Reagents: Potassium carbonate , Sodium sulfate Catalysts: Copper Solvents: Nitrobenzene ; 200 °C

参考文献：

Carbazole compounds for organic electronic device

, Korea, , ,

合成路线：1 步