957476-07-2 ((N1,N2-Bis(2,4,6-trimethoxyphenyl)ethanediamide)

_93%

反应条件：

1.1 Reagents: Triethylamine Solvents: Tetrahydrofuran ; 0 °C; 0 °C → rt; 2 h, rt

参考文献：

Preparation of oxalic acid monoamide ligand compounds for catalysis of coupling reactions

, World Intellectual Property Organization, , ,

合成路线：1 步

_93%

反应条件：

1.1 Reagents: Triethylamine Solvents: Tetrahydrofuran ; 0 °C; 2 h, rt

参考文献：

CuI/Oxalamide Catalyzed Couplings of (Hetero)aryl Chlorides and Phenols for Diaryl Ether Formation

Fan, Mengyang; Zhou, Wei; Jiang, Yongwen; Ma, Dawei, Angewandte Chemie, 2016, 55(21), 6211-6215

合成路线：1 步

_93%

反应条件：

1.1 Reagents: Triethylamine Solvents: Tetrahydrofuran ; 0 °C; 2 h, rt

参考文献：

Assembly of Primary (Hetero)Arylamines via CuI/Oxalic Diamide-Catalyzed Coupling of Aryl Chlorides and Ammonia

Fan, Mengyang; Zhou, Wei; Jiang, Yongwen; Ma, Dawei, Organic Letters, 2015, 17(23), 5934-5937

合成路线：1 步

_93%

反应条件：

1.1 Reagents: Triethylamine Solvents: Tetrahydrofuran ; 0 °C; 2 h, rt
1.2 Solvents: Water ; rt

参考文献：

CuI/Oxalic Diamide Catalyzed Coupling Reaction of (Hetero)Aryl Chlorides and Amines

Zhou, Wei; Fan, Mengyang; Yin, Junli; Jiang, Yongwen; Ma, Dawei, Journal of the American Chemical Society, 2015, 137(37), 11942-11945

合成路线：1 步

_91%

反应条件：

1.1 Reagents: Triethylamine Solvents: Tetrahydrofuran ; 0 °C; 2 h, rt

参考文献：

Co-catalytic borinate enables air-tolerant copper/oxalamide catalysis for cost-effective hydroxylation of aryl bromides

Tao, Shujing; Xu, Minling; Zou, Gang, Tetrahedron Letters, 2023, 123,

合成路线：1 步

_91%

反应条件：

1.1 Reagents: Triethylamine Solvents: Tetrahydrofuran ; 0 °C; 2 h, rt

参考文献：

Copper-Catalyzed Coupling Reaction of (Hetero)Aryl Chlorides and Amides

De, Subhadip; Yin, Junli; Ma, Dawei, Organic Letters, 2017, 19(18), 4864-4867

合成路线：1 步

_91%

反应条件：

1.1 Reagents: Triethylamine Solvents: Tetrahydrofuran ; cooled; 2 h, rt

参考文献：

Discovery of N-(Naphthalen-1-yl)-N'-alkyl Oxalamide Ligands Enables Cu-Catalyzed Aryl Amination with High Turnovers

Gao, Jie; Bhunia, Subhajit; Wang, Kailiang; Gan, Lu; Xia, Shanghua; et al, Organic Letters, 2017, 19(11), 2809-2812

合成路线：1 步

_80%

反应条件：

1.1 Reagents: Triethylamine Solvents: Diethyl ether ; 0 °C; overnight, rt

参考文献：

Cyclometalated and Alkoxyphenyl-Substituted Palladium Imidazolin-2-ylidene Complexes. Synthetic, Structural, and Catalytic Studies

Stylianides, Neoklis; Danopoulos, Andreas A.; Pugh, David; Hancock, Fred; Zanotti-Gerosa, Antonio, Organometallics, 2007, 26(23), 5627-5635

合成路线：1 步

反应条件：

1.1 Reagents: Triethylamine Solvents: Tetrahydrofuran ; 0 °C; 0 °C → rt; 2 h, rt

参考文献：

Preparation method of benzimidazole compound in disinfectant and pesticide

, China, , ,

合成路线：1 步

反应条件：

1.1 Reagents: Triethylamine Solvents: Tetrahydrofuran ; 0 °C; 2 h, rt

参考文献：

Decarboxylative C(sp3)-N cross-coupling via synergetic photoredox and copper catalysis

Mao, Runze ; Frey, Adrian; Balon, Jonathan; Hu, Xile, Nature Catalysis, 2018, 1(2), 120-126

合成路线：1 步