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Dissolution of cellulose in the mixed solvent of [bmim]Cl–DMAc and its application
Lianzhen Lin,Hideki Yamaguchi,Ayami Suzuki
RSC Advances Pub Date : 06/13/2013 00:00:00 , DOI:10.1039/C3RA41299G
Abstract

A mixed solvent of 1-butyl-3-methylimidazolium chloride ([bmim]Cl) and dimethylacetamide (DMAc) was developed for various applications involving cellulose. By changing the ratio of DMAc, the mixed solvent could be used either for cellulose swelling (more than 65% DMAc), selective dissolution of the non-crystalline domains for extraction of the crystalline nanofibers of cellulose (35–60% DMAc), or complete dissolution (less than 30% DMAc). In the region of complete dissolution, the dissolution rate of cellulose increased drastically as the DMAc ratio increased. The cellulose nanofibers prepared in the mixed solvent of [bmim]ClDMAc (50% DMAc) had a diameter of 30 nm and maintained the crystalline structure of cellulose I. A model was proposed to describe the selective dissolution and fibrillation of cellulose nanofibers in the mixed solvent of [bmim]ClDMAc.

Graphical abstract: Dissolution of cellulose in the mixed solvent of [bmim]Cl–DMAc and its application
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